Instrumental Analysis: CHEM 3590

Class schedule, Fall 2018  MACHRAY HALL  Rm: 124

Please note: Handouts available from this site are not complete set of notes.

You are expected to complete the notes in class.

 

Class

Date

Topic

Lecturer (default: HP)

 

 

 

 

1

Sept. 5

Intro to course

 

Sept. 7 

Intro to lab (find file in lab section)

 Dr. Tom Ward

 

 

 

 

3

Sept. 10

Equilibrium involving calcium ions

4

Sept. 12

Problem set on equilibrium + multiprotic acids

 

5

Sept. 14 

Spectroscopy in MCAL (find file in lab section)

 Dr. Tom Ward

 

 

 

 

6

Sept. 17

Ca spectrophotometric analysis

 Milan Teraiya

7

Sept. 19

UV-vis questions and ICP-OES

 

8

Sept. 21

ICP-OES

 

 

 

 

 

9

Sept. 24

ICP-OES questions + Water hardness tests

 

10

Sept. 26

XPS

 

11

Sept. 28

SIMS

 

 

 

 

 

 12

Oct. 1

Case study using several techniques

 

 

Oct. 3

Review for Test 1: 2016 test  2017 test

 

 

Oct. 5

Test 1 Answers VA  Answers VB

 

 

 

 

 

Oct. 8

No class (Thanksgiving)

 

13

Oct. 10

VOCs: GC

 

14

Oct. 12

GC: derivatization procedures

 

 

 

 

15

Oct. 15

GC in MCAL

Dr. Tom Ward

16

Oct. 17

GC/MS

17

Oct. 19

HPLC with UV and Fluorescence detection

 

 

 

 

18

Oct. 22

HPLC in MCAL

Dr. Tom Ward

19

Oct. 24

HPLC with Fluorescence detection (cont’d)

 

20

Oct. 26

HPLC/MS and GC/MS in MCAL

Dr. Tom Ward

 

 

 

 

21

Oct. 29

Size exclusion chromatography

 

22

Oct. 31

Ion exchange chromatography

Milan Teraiya

23

Nov. 2

LC detectors other than UV/fluor.

 

 

 

 

24

Nov. 5

Case study using several techniques

 

Nov. 7

Review for Test 2  2015  2016  2017  ans2015 ans2016

Nov. 9

Test 2 Answers

 

 

 

 

Nov. 12

No class

Nov. 14

No class

Nov. 16

No class

 

 

 

 

25

Nov. 19

HPLC-MS interfaces

26

Nov. 21

LC-MS (cont’d)

27

Nov. 23

CE and detectors

 

 

 

 

28

Nov. 26

CE (cont’d)

29

Nov. 28

Intro electrochemistry

 

30

Nov. 30

Voltammetry

 

 

 

 

31

Dec. 3

ICP-MS

 

32

Dec. 5

Treatment of drinking water – focus on As

 

Dec. 7

Review for final 2017  2016  2015   

 2018 final, answers

 

 

Answers 2017  Answers 2016    Answers 2015